HuagongsheHuagongshe Chemistry Print Report · For research reference only
Adipic Acid → HCID 12892893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Adipic Acid | HCID 196 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12892893 | HCID 12892893 | 115% |
Reaction Steps
To a solution of 7.3 g (0.05 mol) of adipic acid dissolved in 100 ml of methanol, 8.5 g (0.1 mol) of piperidine was added dropwise under stirring, and the precipitate crystals were filtered and dried, to obtain a 13.3 g (yield 55.0%) of adipic acid piperidine salt (molar ratio 1:2) of white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05004787 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-4fd356f5e292499fb4c971ed6aa5fca7 |
| Source note | uspto-grants-1991_04 |