Adipic Acid → HCID 12892893, compound

HRID 1084466Notes

Reaction equation

HRID 1084466 reaction equation
[C:1]([OH:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([OH:8])=[O:7].[NH:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1>CO>[NH:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1.[C:1]([OH:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([OH:8])=[O:7]

Participants

4

Reactant 2

HCID 196Adipic AcidHCID 8082Piperidine

Product 1

HCID 12892893HCID 12892893, compoundYield 115%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a solution of 7.3 g (0.05 mol) of adipic acid dissolved in 100 ml of methanol, 8.5 g (0.1 mol) of piperidine was added dropwise under stirring, and the precipitate crystals were filtered and dried, to obtain a 13.3 g (yield 55.0%) of adipic acid piperidine salt (molar ratio 1:2) of white crystals.

Workup

  1. filtrationthe precipitate crystals were filtered
  2. customdried

Sources & evidence

ORD record
ord-4fd356f5e292499fb4c971ed6aa5fca7
Source dataset
uspto-grants-1991_04
Patent number
US05004787

Reaction notes

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