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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1084678Generated: November 2, 2026

Isopropanol → HCID 15702299, compound

https://huagongshe.com/reaction/1084678

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsopropanolHCID 3776—
ReactantAmmonium ChlorideHCID 25517—
ReactantHCID 15702298HCID 15702298—
CatalystIronHCID 23925—
SolventWaterHCID 962—
ProductHCID 15702299HCID 15702299—

Reaction Steps

Thereafter, the nitro compound was added to 300 ml of isopropyl alcohol with the addition of 30 ml of water and 3 g of ammonium chloride followed by reflux for 2 hours with the addition of 30 g of reducing iron and then the reflux liquid was filtered and the solid precipitated upon cooling the filtrate was filtered to obtain 4.2 g of 1-(2'-hydroxymethylbenzoyl)-2-(p-aminophenyl)hydrazine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05006445
Source datasetuspto-grants-1991_04
ORD IDord-b11310d77cb448e192283f01a547e2e3
Source noteuspto-grants-1991_04