HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,11-Dihydro-11-[4-(1-piperidinyl)-but-2-ynyl]-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → 5,11-Dihydro-11-[4-(1-piperidinyl)butyl]-6H-pyrido[2,3-b][l,4]benzodiazepin-6-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,11-Dihydro-11-[4-(1-piperidinyl)-but-2-ynyl]-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 14552090 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 5,11-Dihydro-11-[4-(1-piperidinyl)butyl]-6H-pyrido[2,3-b][l,4]benzodiazepin-6-one | HCID 14552101 | 35% |
Reaction Steps
Prepared analogously to Example 8 from 5,11-dihydro-11-[4-(1-piperidinyl)-but-2-ynyl]-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one in a yield of 35% of theory. Colourless crystals, m.p. 131°-132° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05006522 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-ca07fb1ce11140b19bd4b6c1c1513129 |
| Source note | uspto-grants-1991_04 |