Hydrochloric Acid → HCID 14328079, compound

HRID 1084775Notes

Reaction equation

HRID 1084775 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[CH:20]=[CH:19][C:14]3[NH:15][C:16](=[O:18])[O:17][C:13]=3[CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:21]>CO>[ClH:21].[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[CH:20]=[CH:19][C:14]3[NH:15][C:16](=[O:18])[O:17][C:13]=3[CH:12]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 143280786-[(3-Phenylpropyl)amino]-1,3-benzoxazol-2(3H)-one

Product 1

HCID 14328079HCID 14328079, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A methanol solution (40 ml) containing 3.06 g of 6-(3-Phenylpropylamino)-2-benzoxazolone was combined with an ethereal solution saturated with gaseous hydrogen chloride (40 ml) at ice-bath temperature. The resulting solid was collected by filtration, washed with ether and dried to give the title compound (3.470 g).

Workup

  1. filtrationThe resulting solid was collected by filtration
  2. washwashed with ether
  3. customdried

Sources & evidence

ORD record
ord-a9831ae8443a4050bf59c413cdada7d9
Source dataset
uspto-grants-1991_04
Patent number
US05006541

Reaction notes

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