Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-tert-Butylcyclohexylamine | HCID 103920 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14795572 | HCID 14795572 | — |
Reaction Steps
A mixture consisting of 13.2 ml of 10N hydrochloric acid, 50 ml of water, 18.8 g of tert.-butyl-cyclohexyl-amine and 17.9 g of sodium nitrite is heated at 90° C. for 3 hours. On cooling, a solid precipitates and is filtered off with suction. Yield: 16.3 g melting point: 87° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05006540 |
|---|
| Source dataset | uspto-grants-1991_04 |
|---|
| ORD ID | ord-77aa9f8eb74141e79be38cc3de5af618 |
|---|
| Source note | uspto-grants-1991_04 |
|---|
