Hydrochloric Acid → HCID 14795572, compound

HRID 1084782Notes

Reaction equation

HRID 1084782 reaction equation
Cl.[C:2]([NH:6][CH:7]1[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1)([CH3:5])([CH3:4])[CH3:3].[N:13]([O-])=[O:14].[Na+]>O>[N:13]([N:6]([C:2]([CH3:5])([CH3:3])[CH3:4])[CH:7]1[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1)=[O:14]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 103920N-tert-ButylcyclohexylamineHCID 23668193Sodium Nitrite

Product 1

HCID 14795572HCID 14795572, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
90 °C

Procedure

A mixture consisting of 13.2 ml of 10N hydrochloric acid, 50 ml of water, 18.8 g of tert.-butyl-cyclohexyl-amine and 17.9 g of sodium nitrite is heated at 90° C. for 3 hours. On cooling, a solid precipitates and is filtered off with suction. Yield: 16.3 g melting point: 87° C.

Workup

  1. temperatureOn cooling
  2. customa solid precipitates
  3. filtrationis filtered off with suction

Sources & evidence

ORD record
ord-77aa9f8eb74141e79be38cc3de5af618
Source dataset
uspto-grants-1991_04
Patent number
US05006540

Reaction notes

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