HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 20062389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | Diethyl vinylphosphonate | HCID 69629 | — |
| Reactant | 4-Chloro-benzaldehyde oxime | HCID 219158 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 20062389 | HCID 20062389 | 102.8% |
Reaction Steps
The compound is prepared in analogy to Example 1 from 23.34 g (0.15 mol) of 4-chlorobenzaldoxime, 22 g of N-chlorosuccinimide, 27.1 g of diethyl vinylphosphonate and 22.9 ml of triethylamine, resulting in 49 g of oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05006515 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-9d7780b8adc445269464f56b9b3bd97e |
| Source note | uspto-grants-1991_04 |