HRID1084791

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID31398

N-Chlorosuccinimide

C4H4ClNO2

HCID69629

Phosphonic acid, vinyl-, diethyl ester

C6H13O3P

HCID219158

4-Chlorobenzaldehyde oxime

C7H6ClNO

PRODUCTS

产物

反应SMILES：CCOP(=O)(OCC)C1CC(c2ccc(Cl)cc2)=NO1

HCID20062389

未命名化合物

收率 102.8%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

The compound is prepared in analogy to Example 1 from 23.34 g (0.15 mol) of 4-chlorobenzaldoxime, 22 g of N-chlorosuccinimide, 27.1 g of diethyl vinylphosphonate and 22.9 ml of triethylamine, resulting in 49 g of oily product.