化工社化工社 化学情報印刷レポート · 研究参考用
Diethyl 3-tert.butyl-2-isoxazolin-5-ylphosphonate → (3-tert-Butyl-4,5-dihydro-1,2-oxazol-5-yl)phosphonic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethyl 3-tert.butyl-2-isoxazolin-5-ylphosphonate | HCID 86744708 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 溶媒 | Hydrogen Bromide | HCID 260 | — |
| 生成物 | (3-tert-Butyl-4,5-dihydro-1,2-oxazol-5-yl)phosphonic acid | HCID 3079426 | — |
反応手順
39.6 g (0.15 mol) of the compound from Example 26 are dissolved in a mixture of 100 ml of 33% strength HBr/glacial acetic acid solution and 50 ml of glacial acetic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05006515 |
| 出典データセット | uspto-grants-1991_04 |
| ORD ID | ord-f24c5b647cdf46038b1a56e6c3513a51 |
| 出典メモ | uspto-grants-1991_04 |