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HRID1084804

反应详情

EQUATION

反应方程式

HRID 1084804 的结构方程式

REACTANTS

反应物

4
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C1CCC(=O)N1Cl
HCID31398

N-Chlorosuccinimide

C4H4ClNO2

结构：C=CP(=O)(OC)OC
HCID78376

Dimethyl vinylphosphonate

C4H9O3P

结构：O=[N+]([O-])c1ccc(C=NO)cc1
HCID96339

N-[(4-Nitrophenyl)methylidene]hydroxylamine

C7H6N2O3

PRODUCTS

生成物

1
结构：COP(=O)(OC)C1CC(c2ccc([N+](=O)[O-])cc2)=NO1
HCID14460583

未命名化合物

PROCEDURE

实验过程

Preparation is carried out in analogy to Example 1 from 19.6 g (0.118 mol) of 4-nitrobenzaldoxime, 17.4 g (0.13 mol) of N-chlorosuccinimide, 16.1 g (0.118 mol) of dimethyl vinylphosphonate and 18.7 ml (0.13 mol) of triethylamine. Crystallization of the crude product from tert.butyl methyl ether provides analytically pure compound of melting point 156° to 158° C.

WORKUP

后处理

  1. customPreparation
  2. customCrystallization of the crude product from tert.butyl methyl ether
  3. customprovides analytically pure compound of melting point 156° to 158° C.