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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1084839Generated: October 29, 2026

3-Chloro-1-propanol → Diisopropylether ethyl acetate

https://huagongshe.com/reaction/1084839

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Chloro-1-propanolHCID 12313—
ReactantHCID 14796259HCID 14796259—
ProductDiisopropylether ethyl acetateHCID 22281796—

Reaction Steps

By reacting in the same manner as in Example 1, using 4 g of 1-(4-hydroxyphenyl)-3-phenyl-1H-pyrazolo[3,4-b]pyridine and 3.6 g of 3-chloropropanol and recrystallizing the obtained crude crystals from ethyl acetate-isopropyl ether, there was obtained 1-[4-(3-hydroxypropoxy)phenyl]-3-phenyl-1H-pyrazolo[3,4-b]pyridine, m.p. 135°-138° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05006520
Source datasetuspto-grants-1991_04
ORD IDord-ac520d75b54f4dbda0a8e1328e94b3d6
Source noteuspto-grants-1991_04