HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 86744718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Maleate(2-) | HCID 5288227 | — |
| Reactant | HCID 15158086 | HCID 15158086 | — |
| Product | HCID 86744718 | HCID 86744718 | — |
Reaction Steps
By conducting reactions and treatments in the same manner as in Example 42, using 5.8 g of 2-chloro-3-[4-(2-dimethylaminoethylamino)benzoyl]pyridine and 1.2 g of methylhydrazine, converting into the maleate and recrystallizing from ethyl acetate, there was obtained 1-methyl-3-[4-(2-dimethylaminoethylamino)phenyl]-1H-pyrazolo[3,4-b]pyridine·maleate, m.p. 88°-90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05006520 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-4de5f8173d42477aa617ac5b9eeb5802 |
| Source note | uspto-grants-1991_04 |