2,5-Hexanedione → HCID 85614082, compound

HRID 1084898Notes

Reaction equation

HRID 1084898 reaction equation
Cl.[C:2]([NH:6][NH2:7])([CH3:5])([CH3:4])[CH3:3].[CH3:8][C:9](=O)[CH2:10][CH2:11][C:12](=O)[CH3:13]>>[C:2]([NH:6][N:7]=[C:9]([CH2:10][CH2:11][C:12](=[N:7][NH:6][C:2]([CH3:5])([CH3:4])[CH3:3])[CH3:13])[CH3:8])([CH3:5])([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 80352,5-HexanedioneHCID 81889tert-Butylhydrazine monohydrochloride

Product 1

HCID 85614082HCID 85614082, compoundYield 60%

Procedure

The procedure of Example (a) is followed using about 67.6 g (0.54 mole) of t-butyl hydrazine hydrochloride and about 28.5 g (0.25 mole) of 2,5-hexane-di-one. The title compound is isolated as a fraction distilled at about 106° C.-114° C. under 1.0 mm Hg pressure. The yield is about 60 percent based upon the initial amount of hexane-di-one.

Sources & evidence

ORD record
ord-ee16e677f291467180daa61c3b0ad4a7
Source dataset
uspto-grants-1991_04
Patent number
US05006567

Reaction notes

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