2,5-Hexanedione → HCID 85614082, compound

Participants

Reaction Steps

The procedure of Example (a) is followed using about 67.6 g (0.54 mole) of t-butyl hydrazine hydrochloride and about 28.5 g (0.25 mole) of 2,5-hexane-di-one. The title compound is isolated as a fraction distilled at about 106° C.-114° C. under 1.0 mm Hg pressure. The yield is about 60 percent based upon the initial amount of hexane-di-one.

Provenance & Evidence