Acetophenone → HCID 136372, compound

HRID 1084899Notes

Reaction equation

HRID 1084899 reaction equation
[C:1]1([NH:7][NH2:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:9]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)(=O)[CH3:10]>>[C:1]1([NH:7][N:8]=[C:9]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH3:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 7410AcetophenoneHCID 7516Phenylhydrazine

Product 1

HCID 136372HCID 136372, compound

Conditions

Temperature
15 °C

Procedure

Phenylhydrazine (10.8 g, 0.10 mole) is added to 20 g (0.10 mole) of acetophenone with stirring at about 15° C. The reaction produces a slight exotherm and the solution solidifies. The title product is allowed to sit for about 12 hours at room temperature and is then used without further purification.

Workup

  1. customThe reaction produces a slight exotherm

Sources & evidence

ORD record
ord-3a13b753e9a442b3a9c97f7b70d9333d
Source dataset
uspto-grants-1991_04
Patent number
US05006567

Reaction notes

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