2-[N-Methyl-N-(2-{4-nitrophenoxy}ethyl)amino]-5-nitroindane → HCID 14835240, compound

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Reaction Steps

A solution of 2-[N-methyl-N-(2-{4-nitrophenoxy}ethyl)amino]-5-nitroindane (0.3 g) in ethyl acetate (30 ml) containing 5% Pd/C (0.03 g) was stirred under a hydrogen atmosphere [206.8 kPa (30 p.s.i.)] for 2 hours at room temperature. The catalyst was then removed by filtration and the filtrate evaporated in vacuo to afford the title compound as a gum, yield 0.25 g, which was used directly without further purification.

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