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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1084935Generated: October 31, 2026

1-(1-Cyclohexen-1-ylmethyl)pyrrolidine-2-methylamine → HCID 13983532, compound

https://huagongshe.com/reaction/1084935

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(1-Cyclohexen-1-ylmethyl)pyrrolidine-2-methylamineHCID 3018317—
ReactantHCID 20062899HCID 20062899—
SolventMethyl Ethyl KetoneHCID 6569—
ProductHCID 13983532HCID 13983532—

Reaction Conditions

Temperature5 °C

Reaction Steps

101 g of 1-cyclohexenylmethyl-2-aminomethylpyrrolidine and 200 ml of methyl ethyl ketone were introduced into a 2-liter round-bottomed flask. The contents were cooled to 5° C. and a solution of 109 g of 6-chlorochroman-8-carbonyl chloride in 500 ml of methyl ethyl ketone was added dropwise, while maintaining the temperature between 0° and 5° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05006570
Source datasetuspto-grants-1991_04
ORD IDord-40621e3631d946a6a79de0467ecbc44f
Source noteuspto-grants-1991_04