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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1084938Generated: November 1, 2026

Chlorosulfonic acid → HCID 20062884, compound

https://huagongshe.com/reaction/1084938

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChlorosulfonic acidHCID 24638—
ReactantHCID 14838687HCID 14838687—
ProductHCID 20062884HCID 20062884—

Reaction Conditions

Temperature50 °C

Reaction Steps

218 g of chlorosulphonic acid were introduced into a 500 ml round-bottomed flask and 65 g of finely ground 4-methoxy-2-methyl-2,3-dihydrobenzofuran-7-carboxylic acid were added in small amounts. The temperature rose to 38° C. The contents were then heated to 50° C. After cooling, the solution obtained was poured, in small amounts, onto ice, with stirring.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05006570
Source datasetuspto-grants-1991_04
ORD IDord-9a97aa7b0c3a40a982a79f6a72f6e42a
Source noteuspto-grants-1991_04