huagongshe.com
HRID1084966

反应详情

EQUATION

反应方程式

HRID 1084966 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=O)c1ccc(I)cc1
HCID879933

4-iodo-N,N-dimethylbenzamide

C9H10INO

结构：C#CCOCCCCCCNCc1ccccc1
HCID19101838

N-Benzyl-6-[(prop-2-yn-1-yl)oxy]hexan-1-amine

C16H23NO

PRODUCTS

生成物

1
结构：CN(C)C(=O)c1ccc(C#CCOCCCCCCNCc2ccccc2)cc1
HCID20062820

未命名化合物

收率 83%

PROCEDURE

实验过程

From 4-iodo-N,N-dimethylbenzamide (2.5 g) and N-[6-[(2-propynyl)oxy]-hexyl]benzenemethanamine (2.23 g). FCC purification eluting with ethyl acetate-triethylamine (100:1) gave the title compound as an orange oil (2.96 g), t.l.c. (Ethyl acetate+few drops triethylamine) Rf 0.15.

WORKUP

后处理

  1. customFCC purification
  2. washeluting with ethyl acetate-triethylamine (100:1)