HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-iodo-N,N-dimethylbenzamide → HCID 20062820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-iodo-N,N-dimethylbenzamide | HCID 879933 | — |
| Reactant | N-Benzyl-6-[(prop-2-yn-1-yl)oxy]hexan-1-amine | HCID 19101838 | — |
| Product | HCID 20062820 | HCID 20062820 | 83% |
Reaction Steps
From 4-iodo-N,N-dimethylbenzamide (2.5 g) and N-[6-[(2-propynyl)oxy]-hexyl]benzenemethanamine (2.23 g). FCC purification eluting with ethyl acetate-triethylamine (100:1) gave the title compound as an orange oil (2.96 g), t.l.c. (Ethyl acetate+few drops triethylamine) Rf 0.15.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05006556 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-2ba52b13402c430795a26e8519809546 |
| Source note | uspto-grants-1991_04 |