HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Chloromethyl)-4-methoxy-5-methylpyridine → 2[(4-Methoxy-5-methylpyridin-2-yl)methylthio]-6-methyl-3-phenyl-4(3H)-quinazolinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Chloromethyl)-4-methoxy-5-methylpyridine | HCID 14479914 | — |
| Reactant | HCID 178423443 | HCID 178423443 | — |
| Product | 2[(4-Methoxy-5-methylpyridin-2-yl)methylthio]-6-methyl-3-phenyl-4(3H)-quinazolinone | HCID 14575170 | 32.9% |
Reaction Steps
The title compound was prepared in a yield of 32.9%, using 2-mercapto-6-methyl-3-phenyl-4(3H)-quinazolinone in place of 2-mercapto-3-phenyl-4(3H)-quinazolinone and 2-chloromethyl-4-methoxy-5-methylpyridine in place of 2chloromethyl-4-methylpyridine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05008266 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-dfd72a80dcb34bd8bbc072c2038e9d70 |
| Source note | uspto-grants-1991_04 |