HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178467921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Reactant | HCID 20061015 | HCID 20061015 | — |
| Product | HCID 178467921 | HCID 178467921 | — |
Reaction Steps
A solution of the aniline from Example 14 (0.38 g, 1 mmol) and glacial acetic acid (0.5 ml) in triethyl orthoacetate (5 ml) was stirred at 25° C. for 72 hours. The product was filtered and recrystallised from toluene (60 mg, 13%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05008263 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-1ebb9be81874448f97c22567c2620966 |
| Source note | uspto-grants-1991_04 |