Methacrylic Acid → HCID 86588650, compound

Participants

Reaction Steps

To a solution of 113.4 g of allyl methacrylate and 8.6 g of methacrylic acid dissolved in 2 liters of 1,2-dichloroethane was added 1.8 g of 2,2'-azobis(2,4-dimethylvaleronitrile) as the polymerization initiator and the mixture was refluxed for 5 hours. After refluxing, the reaction mixture was concentrated under reduced pressure and the concentrate was poured into hexane, followed by drying of the precipitates obtained under vacuum to obtain a binder 1.

Provenance & Evidence