HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 15056302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,6-Dichloro-4-mercaptophenol | HCID 3016363 | — |
| Reactant | HCID 15056293 | HCID 15056293 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15056302 | HCID 15056302 | — |
Reaction Steps
1-(1-Oxo-2-propenyl)-4-(phenylmethyl)piperazine (2.53 g, 0.011 mole) and 2,6-dichloro-4-mercaptophenol (2.15 g, 0.011 mole) were dissolved in methanol (75 ml). Triethylamine (1 ml) was added and the reaction stirred for 12 hours. The solvent was removed, and the product purified by chromatography on silica, eluting with ethyl acetate/hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05010080 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-7945b37c026243a9bdf025f4cf1f6c65 |
| Source note | uspto-grants-1991_04 |