HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 20060099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 19804698 | HCID 19804698 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20060099 | HCID 20060099 | — |
Reaction Steps
3.0 g of 2-chloro-4-methyl-6-cyclopropylpyrimidine are dissolved in 30 ml of ethanol; 3.8 ml of hydrazine hydrate are added and the mixture is stirred for 20 hours at room temperature. The solvent is then evaporated off in vacuo and the residue is recrystallised with ethyl acetate. M.p. 98°-99° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05010082 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-80d05987f4c04b3f87a30da479f6ac04 |
| Source note | uspto-grants-1991_04 |