Hydrochloric Acid → FK 336

HRID 1085499Notes

Reaction equation

HRID 1085499 reaction equation
[N+:1]([O:4][CH2:5][CH2:6][NH:7][C:8]([C:10]1[N:11]=[C:12]([CH3:15])[S:13][CH:14]=1)=[O:9])([O-:3])=[O:2].[ClH:16]>>[ClH:16].[N+:1]([O:4][CH2:5][CH2:6][NH:7][C:8]([C:10]1[N:11]=[C:12]([CH3:15])[S:13][CH:14]=1)=[O:9])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 1294034-Thiazolecarboxamide, 2-methyl-N-[2-(nitrooxy)ethyl]-

Product 1

HCID 129402FK 336

Procedure

IR (Nujol): 3280, 3135, 1647, 1618, 1545, 1278 cm-1 (c) N-(2-Nitrooxyethyl)-2-methyl-4-thiazolecarboxamide was transformed into its hydrochloride in a conventional manner, followed by recrystallization from ethanol to obtain white crystals of N-(2-nitrooxyethyl)-2-methyl-4-thiazolecarboxamide hydrochloride.

Workup

  1. customfollowed by recrystallization from ethanol

Sources & evidence

ORD record
ord-a03e11addadc40858e4916bda447788c
Source dataset
uspto-grants-1991_04
Patent number
US05010093

Reaction notes

Loading…