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HRID1085622

反应详情

EQUATION

反应方程式

HRID 1085622 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1
HCID169132

Isophorone diisocyanate

C12H18N2O2

结构：CC(N)COCC(C)OCC(C)OCC(C)N
HCID15131492

未命名化合物

PRODUCTS

生成物

1
结构：CC(N)COCC(C)OCC(C)OCC(C)N.CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1
HCID131716334

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

A mixture of JEFFAMINE® D-400 (160 g, 0.40 m) and i-PrOH (120) was charged into a flask. Isophorone diisocyanate (44.4 g, 0.20) was added dropwise at 20°-25° C. over a 1 hour period of time. The solvent in the product solution was removed by using a high vacuum. The resulting product was a colorless semisolid at room temperature. The analysis of amine indicated 1.59 meq/g.

WORKUP

后处理

  1. additionwas charged into a flask
  2. customThe solvent in the product solution was removed
  3. customat room temperature