HRID1085642

反应详情

EQUATION

反应方程式

HRID 1085642 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2,6-Dimethylphenylisocyanate (1.5 g) was added dropwise to a solution of N-isopropylhexahydropyrimidine (1.3 g) in acetonitrile (5 ml) (exothermic). After cooling the title compound was isolated by filtration and recrystallised from acetonitrile (2,5 g, 89%), mp 138°-139° C.