HRID1085757

反应详情

EQUATION

反应方程式

HRID 1085757 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

10.6 g of 4'-hydroxybiphenyl-4-carboxylic acid and 18.7 g of (+)-2-methylbutanol were heat-refluxed for 20 hours in benzene together with 1 ml of sulfuric acid. The mixture was subjected to filtration, condensation acid recrystallization to obtain 11.0 g of the objective product (yield: 83%).

WORKUP

后处理

  1. filtrationThe mixture was subjected to filtration, condensation acid recrystallization