HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-iodobenzoate → HCID 19768519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-iodobenzoate | HCID 69258 | — |
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 19768519 | HCID 19768519 | 84.5% |
Reaction Steps
52.5 g (0.2 mol) of methyl 3-iodobenzoate were heated to reflux for 18 hours with 81 g (0.2 mol) of Lawesson reagent in 330 ml of xylene. By working-up in an analogous manner to that described in Example 1(B) there were obtained 47 g (84.4%) of O-methyl 3-iodothiobenzoate as a yellow evil-smelling oil which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011849 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-363fa08194634b6280b5403a107ec2ca |
| Source note | uspto-grants-1991_04 |