HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 14717227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 2-Amino-4,6-difluoropyrimidine | HCID 1201480 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Product | HCID 14717227 | HCID 14717227 | — |
Reaction Steps
29.4 g (0.3 mol) of potassium isopropylate were reacted as in 1.2 with 39.3 g (0.3 mol) of 2-amino-4,6-difluoropyrimidine (A.1a) in a total of 400 ml of isopropanol. After the working up, washing with petroleum ether and water in the usual manner, 38.5 g (75% of theory) of the title compound of melting point 66°-68° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011927 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-660f9e644dab46dba9c48fe78b04d4d0 |
| Source note | uspto-grants-1991_04 |