Heptanol → HCID 14717231, compound

Participants

Reaction Steps

A solution of 1.14 g (0.038 mol) of 80% sodium hydride (suspension in linseed oil) in 30 ml of n-heptanol was added to a stirred mixture of 5 g (0.038 mol) of 2-amino-4,6-difluoropyrimidine in 70 ml of n-heptanol at 20° to 25° C. within 5 minutes. After 2.5 hours working up was carried out as in Example 6. 6.3 g (73% of theory) of the title compound of melting point 30°-32° C. were obtained in this way.

Provenance & Evidence