HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 72273890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 77374747 | HCID 77374747 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 72273890 | HCID 72273890 | — |
Reaction Steps
A solution of the benzyl ether 4, 80 ml of acetic acid and 20 ml of water in 50 ml of THF was stirred at 70° C. overnight. The solution was then concentrated under vacuum and the residue purified by chromatography over silica gel (3 EtOAc: 2 hexanes) to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011943 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-eabf241e26a14d6cae9824d7d817e58d |
| Source note | uspto-grants-1991_04 |