HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoylhydrazine → HCID 53876524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoylhydrazine | HCID 11955 | — |
| Reactant | 1-(3-Pyridyl)propan-1-one | HCID 74074 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53876524 | HCID 53876524 | 80.4% |
Reaction Steps
A mixture of 6.76 gm (0.05 mole) of 3-propionylpyridine, 6.81 gm (0.05 mole) of benzhydrazide and 100 ml of absolute ethanol is refluxed 8.5 hr. The hot solution is filtered. The filtrate is cooled to room temperature and then chilled. The crystals that separate are collected and dried to yield 10.18 gm (80%) of the title compound having a melting point of 169.4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011932 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-90034a4423a94f56a8dbc194bdba5b32 |
| Source note | uspto-grants-1991_04 |