HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzoylpyridine → HCID 54141737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzoylpyridine | HCID 26731 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54141737 | HCID 54141737 | 12% |
Reaction Steps
To 6.61 gm (0.05 mole) of t-butylcarbazate dissolved in 100 ml of warm water is added 9.16 gm (0.05 mole) of 4-benzoylpyridine in 30 ml of ethanol. The mixture is refluxed 7 hr. Cooling several weeks yields 1.77 gm (12%) of the title compound having a melting point of 134.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011932 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-cde0f8e43ee441b68ae8352947b7fea7 |
| Source note | uspto-grants-1991_04 |