HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67861287, compound → HCID 178500829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67861287 | HCID 67861287 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178500829 | HCID 178500829 | — |
Reaction Steps
1.0 g of the product from Example 2 was dissolved in methanol, 0.5 g of Raney nickel was added and hydrogenation was carried out under normal pressure at room temperature for four hours. The catalyst was separated off, the solution which remained was evaporated and the evaporation residue was recrystallized from i-propanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011971 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-ace8fa7e493f4bf69459bca87010b08a |
| Source note | uspto-grants-1991_04 |