p-Toluenesulfonic acid → HCID 178500761, compound

HRID 1085985Notes

Reaction equation

HRID 1085985 reaction equation
[NH2:1][CH:2]=[C:3]([C:8](=[O:18])[C:9]1[CH:14]=[C:13]([F:15])[C:12]([F:16])=[CH:11][C:10]=1[Cl:17])[C:4]([O:6][CH3:7])=[O:5].[F:19][C:20]1[CH:26]=[CH:25][C:23](N)=[CH:22][CH:21]=1.C1(C)C=CC(S(O)(=O)=O)=CC=1>O>[Cl:17][C:10]1[CH:11]=[C:12]([F:16])[C:13]([F:15])=[CH:14][C:9]=1[C:8]([C:3](=[CH:2][NH:1][C:23]1[CH:25]=[CH:26][C:20]([F:19])=[CH:21][CH:22]=1)[C:4]([O:6][CH3:7])=[O:5])=[O:18]

Participants

5

Reactant 3

HCID 6101p-Toluenesulfonic acidHCID 97314-FluoroanilineHCID 178500829HCID 178500829, compound

Product 1

HCID 178500761HCID 178500761, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The preparation was carried out analogously to Example 10 with 1.0 g of the product from Example 5, 1.01 g of p-fluoroaniline and 0.69 g of p-toluenesulphonic acid.H2O.

Sources & evidence

ORD record
ord-726a597480dd46a4a87d0d3bf17e23d4
Source dataset
uspto-grants-1991_04
Patent number
US05011971

Reaction notes

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