HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 178455924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 178455925 | HCID 178455925 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178455924 | HCID 178455924 | — |
Reaction Steps
31.5 ml of diethylamine are added to a solution of 21 g (30 mmol) of Fmoc-Val-Arg-Ile-OBzl in 200 ml of dimethylformamide. The mixture is left to stand at room temperature for 10 minutes, and is concentrated in vacuo. The residue is triturated with diethyl ether and filtered off with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05011825 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-13a7e8668c1f49ed8ccba1ad01d60636 |
| Source note | uspto-grants-1991_04 |