Diethylamine → HCID 178446035, compound

Participants

Reaction Steps

12.05 ml of diethylamine are added to a solution of 8.04 g (11.5 mmol) of Fmoc-D-Leu-Arg-D-Val-OBzl in 60 ml of dimethylformamide. The mixture is left to stand at room temperature for 15 minutes, and is concentrated. The residue is partitioned between n-pentanol and NaHCO3 solution. The pentanol phase is concentrated, and the residue is triturated with diethyl ether.

Provenance & Evidence