HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene Oxide → HCID 53821622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene Oxide | HCID 7276 | — |
| Reactant | HCID 19826901 | HCID 19826901 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53821622 | HCID 53821622 | — |
Reaction Steps
A solution of 2,5-dibromothiophene-3-ethylamine (31.6 g) and styrene oxide (13.3 g) in acetonitrile (135 ml) was heated under reflux for 24 hours. After standing at room temperature, brown crystals were filtered contaminated by traces of black tar. Recyrstallisation from acetonitrile (45 ml) with carbon treatment gave the title product (m.p. 94°) as tan crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05028602 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-b82aebf604094ef6b9f7fdc63b622b83 |
| Source note | uspto-grants-1991_07 |