HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → Phenylpyruvic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | HCID 10753428 | HCID 10753428 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Phenylpyruvic acid | HCID 997 | 63% |
Reaction Steps
By the same operation as in Example 61 except that 6 ml of 1,4-dioxane was used as the solvent, 2-oxo-3,4-diphenylbutanoic acid formed in a yield of 63 % by the reaction of 0.49 g (3 mmoles) of phenylpyruvic acid with 0.5 ml of benzyl chloride, as determined by NMR spectral analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05028738 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-6d41415247e646ee94947bad41fddfa4 |
| Source note | uspto-grants-1991_07 |