HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromobenzoic acid → Benzoyl chloride, 3-bromo-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromobenzoic acid | HCID 11456 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | Benzoyl chloride, 3-bromo- | HCID 74377 | — |
Reaction Steps
To CHCl3 is added 3-bromobenzoic acid (100 g) and thionyl chloride (109 ml) and refluxed overnight. The remaining thionyl chloride is evaporated off to afford 3-bromobenzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05028629 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-08fc04917caa495f8445d4a2a01c6a91 |
| Source note | uspto-grants-1991_07 |