Methanol → HCID 53939730, compound

Participants

Reaction Steps

In methanol (15 ml) is placed 2-methylthio-5-(3-phenylpropyl)-N-hydroxy-N-methylcinnamamide (0.35 g, 1.02 mmol) prepared according to Example 27. In 3 ml of water is placed oxone (0.94 g, 1.54 mmol) which is added to the methanol solution and stirred at room temperature for 3 days. The reaction mixture is poured into 80 ml of water, then extracted twice with 75 ml portions of ethyl acetate. The organic layers are washed

Provenance & Evidence