Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Ethane, 1-chloro-2-(ethylsulfonyl)- | HCID 101406 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14677075 | HCID 14677075 | — |
Reaction Steps
Gaseous methylamine is passed to saturation (about 30 min) into a solution of 15.7 g of chloroethyl ethyl sulfone in 100 ml of toluene at an internal temperature of 50° C. The mixture is stirred at 50° C. for 3 h, the precipitate is filtered off with suction, and the filtrate is concentrated in a rotary evaporator. The remaining yellow mobile liquid (12.3 g) is reacted without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05030270 |
|---|
| Source dataset | uspto-grants-1991_07 |
|---|
| ORD ID | ord-7ed1fbeb69b444819da3f0b8709dc87d |
|---|
| Source note | uspto-grants-1991_07 |
|---|
