HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromotrimethylsilane → HCID 10039097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | HCID 14773690 | HCID 14773690 | — |
| Product | HCID 10039097 | HCID 10039097 | 25% |
Reaction Steps
60 mg (0.28 mmole) of compound 4a are treated with 4 equivalents (0.15 ml) of trimethylsilylbromide at ambient temperature for 35 min. The compound obtained is purified by silica gel plate chromatography using an ether:pentane mixture (1:6). This gives 16 mg of compound 5d corresponding to a 25% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030628 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-211de8de5dc0442f80c68016e1b092c4 |
| Source note | uspto-grants-1991_07 |