HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dodecanenitrile → HCID 14651795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dodecanenitrile | HCID 17092 | — |
| Reactant | N-Isopropylethylenediamine | HCID 88098 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | HCID 14651795 | HCID 14651795 | 82.3% |
Reaction Steps
18.324 g of Undecyl cyanide, 15.12 g of N-isopropylethylenediamine and 0.5 ml of carbon disulfide were heated at 125° C. for 24 hrs. and worked up as mentioned under Example 23, followed by distillation at 150° C./1.2 mm gave 21.93 g (82.3%) of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030629 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-5be30f23cd2449618966b040ed7cfe5f |
| Source note | uspto-grants-1991_07 |