HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → 1-(2-Carbmethoxyethyl)-2-undecyl-2-imidazoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | 2-Undecylimidazoline | HCID 245858 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-(2-Carbmethoxyethyl)-2-undecyl-2-imidazoline | HCID 15158288 | 72.4% |
Reaction Steps
2.2 g (9.82 mmoles) of 2-undecyl-2-imidazoline and 1.4 g (16.3 mmoles) of methyl acrylate were dissolved in 50 ml of methylene chloride and the solution was heated to reflux. The reaction was followed by glc. The solution was concentrated and the residue was distilled at 160°-170° C./0.1 mm to give 2.2 g (72.4%) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030629 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-c46d2a1cc86b44dd8ee46f2fbb7ca8c9 |
| Source note | uspto-grants-1991_07 |