HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Dodecanoate → HCID 15158289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Dodecanoate | HCID 7800 | — |
| Reactant | 2-[2-(2-aminoethylamino)ethoxy]ethanol | HCID 10329424 | — |
| Product | HCID 15158289 | HCID 15158289 | 50.7% |
Reaction Steps
13.7 g (92.6 mmoles) N-[2-(2-Hydroxyethoxy)ethyl]ethylenediamine and 19.6 g (86 mmoles) of ethyl dodecanoate were mixed and heated in a flask equipped with a Dean-Stark trap. After the separated ethanol and water were distilled off, the residue was kugelrohr distilled at 160°-170° C./0.1 mm to give 13.6 g (50.7%) of crude product. Recrystallization from ethyl acetate/hexane gave white crystalline material, m.p. 58°-60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030629 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-8e006792af9646799a84c0f34df1c2fd |
| Source note | uspto-grants-1991_07 |