反应详情

Following the method of Example 3, 4-picolyl ethylamine (4.27 g, 0.035 mole) was reacted with acryloyl chloride (3.15 g, 0.035 mole) and triethylamine (21 ml) and purified by chromatography on silica. Analysis calc. for C8H12N2 (136.20): Calc.: C, 69.44; H, 7.92; N, 14.72. Found: C, 69.26; H, 7.56; N, 14.59.

1. custompurified by chromatography on silica